3-(TRIMETHYLSILYLETHYNYL)THIOPHENE 97 synthesis
- Product Name:3-(TRIMETHYLSILYLETHYNYL)THIOPHENE 97
- CAS Number:130995-13-0
- Molecular formula:C9H12SSi
- Molecular Weight:180.34
10486-61-0
158 suppliers
$6.00/1g
1066-54-2
468 suppliers
$9.00/10g
130995-13-0
97 suppliers
$14.00/250mg
Yield: 99%
Reaction Conditions:
with bis-triphenylphosphine-palladium(II) chloride;copper(l) iodide;triethylamine in tetrahydrofuran at 20;Inert atmosphere;Schlenk technique;Sonogashira Cross-Coupling;
References:
Weingand, Vanessa;Wurm, Thomas;Vethacke, Vanessa;Dietl, Martin C.;Ehjeij, Daniel;Rudolph, Matthias;Rominger, Frank;Xie, Jin;Hashmi, A. Stephen K. [Chemistry - A European Journal,2018,vol. 24,# 15,p. 3725 - 3728] Location in patent:supporting information