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3-vinylbiphenyl synthesis

11synthesis methods
-

Yield:38383-51-6 91%

Reaction Conditions:

Stage #1: -butyl vinyl ether;biphenyl-2-yl-lithiumwith zirconocene methyl chloride in tetrahydrofuran at -78 - 80; for 3.5 h;
Stage #2: with water in tetrahydrofuran at 20; for 1 h;

References:

Barluenga, José;Fernández, Amadeo;álvarez-Rodrigo, Lucía;Rodríguez, Félix;Fa?anás, Francisco J. [Synlett,2005,# 16,art. no. G19105ST,p. 2513 - 2515]