4-CHLORO-6-METHYL-2,3-DIHYDRO-1H-8-THIA-5,7-DIAZA-CYCLOPENTA[A]INDENE synthesis

2synthesis methods

Product Name:4-CHLORO-6-METHYL-2,3-DIHYDRO-1H-8-THIA-5,7-DIAZA-CYCLOPENTA[A]INDENE
CAS Number:300816-24-4
Molecular formula:C10H9ClN2S
Molecular Weight:224.71

4815-29-6 Synthesis

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 68 percent / t-BuOK / 0.01 h / 120 °C / microwave irradiation
2: oxalyl chloride / 3 h / Heating

References:

Raghu Prasad, Mailavaram;Prashanth, John;Shilpa, Kalghatgi;Pran Kishore, Deb [Chemical and Pharmaceutical Bulletin,2007,vol. 55,# 4,p. 557 - 560]