(Z)-tert-Butyl 2,3,6,7-tetrahydroazepine-1-carboxylate synthesis
- Product Name:(Z)-tert-Butyl 2,3,6,7-tetrahydroazepine-1-carboxylate
- CAS Number:317336-73-5
- Molecular formula:C11H19NO2
- Molecular Weight:197.27
14002-33-6
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317336-73-5
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Yield:-
Steps:
Multi-step reaction with 6 steps
1.1: Et3N / methanol / 2 h / Heating
2.1: pyridine / CH2Cl2 / 20 °C
3.1: LiBr / acetone / Heating
4.1: sodium sulfide nonahydrate / ethanol / Heating
5.1: N-chlorosuccinimide / CCl4 / 3 h / Heating
5.2: 20 percent / m-chloroperbenzoic acid / CH2Cl2 / 18 h / 20 °C
6.1: 66 percent / potassium tert-butoxide / tetrahydrofuran; dimethylsulfoxide / 0.17 h / 20 °C
References:
MaGee;Beck [Journal of Organic Chemistry,2000,vol. 65,# 24,p. 8367 - 8371]
1211531-07-5
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317336-73-5
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1000210-73-0
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317336-73-5
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793-19-1
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317336-73-5
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5279-23-2
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317336-73-5
58 suppliers
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