3,8-bis[(trimethylsilyl)ethynyl]-1,10-phenanthroline synthesis
- Product Name:3,8-bis[(trimethylsilyl)ethynyl]-1,10-phenanthroline
- CAS Number:320573-10-2
- Molecular formula:C22H24N2Si2
- Molecular Weight:372.61
100125-12-0
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Yield:320573-10-2 100%
Reaction Conditions:
with copper(l) iodide;N-ethyl-N,N-diisopropylamine;bis-triphenylphosphine-palladium(II) chloride in benzene at 95; for 40 h;Sonogashira coupling;
References:
Ciszek, Jacob W.;Tour, James M. [Tetrahedron Letters,2004,vol. 45,# 13,p. 2801 - 2803]
66-71-7
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