ChemicalBook CAS DataBase List 6-methoxy-2-methyl-1H-benz[de]isoquinoline-1,3(2H)-dione

6-methoxy-2-methyl-1H-benz[de]isoquinoline-1,3(2H)-dione synthesis

4synthesis methods

Product Name:6-methoxy-2-methyl-1H-benz[de]isoquinoline-1,3(2H)-dione
CAS Number:3271-05-4
Molecular formula:C14H11NO3
Molecular Weight:241.24

6-bromo-2-methyl-1H-benz[de]isoquinoline-1,3(2H)-dione

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124-41-4 Synthesis

124-41-4
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6-methoxy-2-methyl-1H-benz[de]isoquinoline-1,3(2H)-dione

3271-05-4
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Yield:-

Reaction Conditions:

with copper(ll) sulfate pentahydrate in methanol;Reflux;

Steps:

2 Example 2

A mixture of 1 eq of compound 1 and 1 eq of sodium methoxide was stirred and refluxed in MeOH. CuSO 4 ?5H 2 O was added as a catalyst. Evaporating the reaction mixture in vacuo, To the residue was added 1 M HCl. Filtration and purification to obtain compound 2; The structural formula of the compound 2 is as follows:

References:

CN109970729,2019,A Location in patent:Paragraph 0029; 0030

124-41-4 Synthesis

124-41-4
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$12.00/25g