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tert-butyl 5-(Methoxy(Methyl)carbaMoyl)pyridin-3-ylcarbaMate synthesis

2synthesis methods
-

Yield:337904-93-5 47%

Reaction Conditions:

with bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride;N-ethyl-N,N-diisopropylamine in dichloromethane;

References:

Nakayama, Kiyoshi;Ishida, Yohei;Ohtsuka, Masami;Kawato, Haruko;Yoshida, Ken-Ichi;Yokomizo, Yoshihiro;Hosono, Shigeru;Ohta, Toshiharu;Hoshino, Kazuki;Ishida, Hiroko;Yoshida, Kumi;Renau, Thomas E.;Leger, Roger;Zhang, Jason Z.;Lee, Ving J.;Watkins, William J. [Bioorganic and Medicinal Chemistry Letters,2003,vol. 13,# 23,p. 4201 - 4204]