1,3-Benzodioxole-4-carboxylic acid, 6-amino-, methyl ester synthesis

3synthesis methods

Product Name:1,3-Benzodioxole-4-carboxylic acid, 6-amino-, methyl ester
CAS Number:33842-32-9
Molecular formula:C9H9NO4
Molecular Weight:195.17

33842-18-1 Synthesis

Methyl 6-broMobenzo[d][1,3]dioxole-4-carboxylate

33842-18-1
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1,3-Benzodioxole-4-carboxylic acid, 6-amino-, methyl ester

33842-32-9
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Yield:33842-32-9 30%

Reaction Conditions:

with copper(l) iodide;ammonia;caesium carbonate in N,N-dimethyl-formamide;acetylacetone at 70; for 12 h;

References:

Hermane, Jekaterina;Eichner, Simone;Mancuso, Lena;Schr?der, Benjamin;Sasse, Florenz;Zeilinger, Carsten;Kirschning, Andreas [Organic and Biomolecular Chemistry,2019,vol. 17,# 21,p. 5269 - 5278] Location in patent:supporting information