Benzenebutanenitrile, 4-chloro-α-(4-chlorophenyl)-γ-oxo- synthesis
- Product Name:Benzenebutanenitrile, 4-chloro-α-(4-chlorophenyl)-γ-oxo-
- CAS Number:344281-01-2
- Molecular formula:C16H11Cl2NO
- Molecular Weight:304.17
1073-67-2
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Yield:344281-01-2 71%
Reaction Conditions:
Stage #1: 2-(4-chlorophenyl)-2-oxoacetic acidwith sodium hydroxide in acetonitrile at 20; for 0.166667 h;Electrochemical reaction;Inert atmosphere;
Stage #2: 1-chloro-4-vinylbenzene;3-oxo-1λ3-benzo[d][1,2]iodaoxole-1(3H)-carbonitrilewith lithium perchlorate in acetonitrile at 25; for 7 h;Molecular sieve;Electrochemical reaction;Inert atmosphere;
References:
Kong, Xianqiang;Chen, Xiaohui;Chen, Yiyi;Cao, Zhong-Yan [Journal of Organic Chemistry,2022,vol. 87,# 11,p. 7013 - 7021]