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3,17-Di-O-acetyl Androsta-5,14,16-triene-3β,17-diol synthesis

1synthesis methods
-

Yield:34635-42-2 51%

Reaction Conditions:

with toluene-4-sulfonic acid in Isopropenyl acetate; for 48 h;Inert atmosphere;Reflux;

References:

Baranovskii;Bolibrukh;Gromak [Russian Journal of General Chemistry,2011,vol. 81,# 9,p. 1877 - 1885] Location in patent:experimental part