1-(4-BROMO-PHENYL)-2,5-DIMETHYL-1H-PYRROLE-3-CARBALDEHYDE synthesis
- Product Name:1-(4-BROMO-PHENYL)-2,5-DIMETHYL-1H-PYRROLE-3-CARBALDEHYDE
- CAS Number:347331-78-6
- Molecular formula:C13H12BrNO
- Molecular Weight:278.14
110-13-4
378 suppliers
$10.00/5g
347331-78-6
13 suppliers
$131.00/1g
Yield:-
Steps:
Multi-step reaction with 2 steps
1.1: toluene-4-sulfonic acid; silica gel / neat (no solvent) / 180 °C / Microwave irradiation
2.1: trichlorophosphate / 0.25 h / 20 °C / Inert atmosphere
2.2: 3 h / 100 °C / Inert atmosphere
References:
Murugesan, Dinakaran;Mital, Alka;Kaiser, Marcel;Shackleford, David M.;Morizzi, Julia;Katneni, Kasiram;Campbell, Michael;Hudson, Alan;Charman, Susan A.;Yeates, Clive;Gilbert, Ian H. [Journal of Medicinal Chemistry,2013,vol. 56,# 7,p. 2975 - 2990]
106-40-1
460 suppliers
$12.00/5g
347331-78-6
13 suppliers
$131.00/1g