ChemicalBook CAS DataBase List 2,4-Dihydroxy-3-formyl-6-methylbenzoic acid methyl ester

2,4-Dihydroxy-3-formyl-6-methylbenzoic acid methyl ester synthesis

9synthesis methods

Product Name:2,4-Dihydroxy-3-formyl-6-methylbenzoic acid methyl ester
CAS Number:34874-90-3
Molecular formula:C10H10O5
Molecular Weight:210.18

4885-02-3 Synthesis

4885-02-3
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$10.00/1g

3187-58-4
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$70.00/50mg

2,4-Dihydroxy-3-formyl-6-methylbenzoic acid methyl ester

34874-90-3
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Yield:34874-90-3 87%

Reaction Conditions:

Stage #1: methyl orsellinatewith titanium tetrachloride in dichloromethane at 0; for 0.166667 h;Inert atmosphere;
Stage #2: Dichloromethyl methyl ether in dichloromethane at 0 - 20; for 1 h;Inert atmosphere;

References:

Dong, Chunmao;Huo, Luqiong;Liu, Hongxin;Lu, Xiuxiang;Qiu, Shengxiang;Tan, Haibo;Wang, Miaomiao;Yang, Bao;Yuan, Yunfei;Zhang, Wenge [Organic Letters,2020] Location in patent:supporting information

4885-02-3 Synthesis

4885-02-3
180 suppliers
$10.00/1g