ChemicalBook CAS DataBase List Diethyl (3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooct-1-yl)phosphonate

Diethyl (3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooct-1-yl)phosphonate synthesis

6synthesis methods

Product Name:Diethyl (3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooct-1-yl)phosphonate
CAS Number:350608-55-8
Molecular formula:C12H14F13O3P
Molecular Weight:484.19

647-42-7 Synthesis

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Diethyl (3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooct-1-yl)phosphonate

350608-55-8
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Yield:-

Steps:

Multi-step reaction with 2 steps
1: triphenylphosphine; bromine / acetonitrile / 5 h / 60 °C / Inert atmosphere
2: 4 h / 150 °C

References:

Lukáč, Miloš;Garajová, Mária;Mrva, Martin;Devínsky, Ferdinand;Ondriska, František;Kubincová, Janka [Journal of Fluorine Chemistry,2014,vol. 164,p. 10 - 17]