352557-26-7 synthesis

4synthesis methods

Product Name:352557-26-7
CAS Number:352557-26-7
Molecular formula:C23H43BrO4
Molecular Weight:463.49

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Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: Ru(OAc)2((R)-MeOBIPHEP); hydrogenchloride / water; methanol / 0.5 h / 20 °C / Autoclave; Sealed tube; Inert atmosphere
1.2: 4.42 h / 80 °C / 22502.3 - 30003 Torr / Autoclave; Sealed tube; Inert atmosphere
2.1: potassium hydrogencarbonate; dmap / water; methanol; toluene / 3.5 h / 11 °C

References:

Schwindt, Mark A.;Fleming, Michael P.;Han, Yeun-Kwei;Hodges, Lewis M.;Johnston, David A.;Micheli, Roger P.;Roberts, Chris R.;Snyder, Roger;Topping, Robert J.;Puentener, Kurt;Scalone, Michelangelo [Organic Process Research and Development,2007,vol. 11,# 3,p. 524 - 533]