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2-Propen-1-one, 1-[1,1'-biphenyl]-4-yl-3-(3,4-dimethoxyphenyl)- synthesis
- Product Name:2-Propen-1-one, 1-[1,1'-biphenyl]-4-yl-3-(3,4-dimethoxyphenyl)-
- CAS Number:36635-79-7
- Molecular formula:C23H20O3
- Molecular Weight:344.4
Yield:-
Reaction Conditions:
with alkali metal hydroxide in ethanol;water;
Steps:
Synthesis of chalcones (3a-d):
General procedure: An equimolar amount of 4-phenyl acetophenone (0.02 mol) and substituted benzaldehyde (0.02 mol) were dissolved in absolute alcohol and 10 % KOH solution was added dropwise with stirring the reaction was continued for 2 h and left overnight. Then the mixture of the reaction was kept overnight in an ice-water to obtain the product. The crude product was recrystallized from ethanol to get the final product (Scheme-I).
References:
Sharma, Anupama;Khaturia, Sarita;Singh, Har Lal [Asian Journal of Chemistry,2021,vol. 33,# 3,p. 531 - 536]
![4'-Bromoacetophenone](/CAS/GIF/99-90-1.gif)
99-90-1
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36635-79-7
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![Phenylboronic acid](/CAS/GIF/98-80-6.gif)
98-80-6
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36635-79-7
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