ChemicalBook CAS DataBase List tert-butyl N-[(3-amino-1H-indazol-6-yl)methyl]carbamate

tert-butyl N-[(3-amino-1H-indazol-6-yl)methyl]carbamate synthesis

6synthesis methods

Product Name:tert-butyl N-[(3-amino-1H-indazol-6-yl)methyl]carbamate
CAS Number:368426-74-8
Molecular formula:C13H18N4O2
Molecular Weight:262.31

452-74-4 Synthesis

452-74-4
287 suppliers
$17.00/25g

tert-butyl N-[(3-amino-1H-indazol-6-yl)methyl]carbamate

368426-74-8
16 suppliers
inquiry

Yield:-

Steps:

Multi-step reaction with 6 steps
1: 94 percent / dimethylformamide / 5 h / Heating
2: 54 percent / NBS; AIBN / CCl₄ / 4.5 h / Heating
3: 91 percent / Cs₂CO₃ / dimethylformamide / 0.5 h / 20 °C
4: NH₂NH₂ / butan-1-ol / 0.08 h / Heating
5: CH₂Cl₂ / 1 h / 20 °C
6: 64 percent / NH₂NH₂ / butan-1-ol / 22 h / Heating

References:

Cui, Jingrong Jean;Araldi, Gian-Luca;Reiner, John E.;Reddy, Komandla Malla;Kemp, Scott J.;Ho, Jonathan Z.;Siev, Daniel V.;Mamedova, Lala;Gibson, Tony S.;Gaudette, John A.;Minami, Nathaniel K.;Anderson, Susanne M.;Bradbury, Annette E.;Nolan, Thomas G.;Semple [Bioorganic and Medicinal Chemistry Letters,2002,vol. 12,# 20,p. 2925 - 2930]

229623-55-6 Synthesis

TERT-BUTYL 4-CYANO-3-FLUOROBENZYLCARBAMATE

229623-55-6
16 suppliers
inquiry

368426-74-8
16 suppliers
inquiry

References

85070-67-3 Synthesis

85070-67-3
211 suppliers
$5.00/1g

368426-74-8
16 suppliers
inquiry

References

222978-03-2 Synthesis

222978-03-2
97 suppliers
inquiry

368426-74-8
16 suppliers
inquiry

References

368426-73-7
66 suppliers
inquiry

368426-74-8
16 suppliers
inquiry

References