trimethyl-[2-(1,10-phenanthrolin-3-yl)ethynyl]silane synthesis
- Product Name:trimethyl-[2-(1,10-phenanthrolin-3-yl)ethynyl]silane
- CAS Number:369390-65-8
- Molecular formula:C17H16N2Si
- Molecular Weight:276.41
66127-01-3
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Yield:369390-65-8 92%
Reaction Conditions:
with copper(l) iodide;triethylamine;bis-triphenylphosphine-palladium(II) chloride in benzene at 80 - 90; for 24 h;Sonogashira coupling;
References:
Schmittel;Michel;Wiegrefe;Kalsani [Synthesis,2001,# 10,p. 1561 - 1567]
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