ChemicalBook CAS DataBase List (4-Oxo-3,4-dihydro-1,5-benzothiazepin-5(2H)-yl)-acetic acid

(4-Oxo-3,4-dihydro-1,5-benzothiazepin-5(2H)-yl)-acetic acid synthesis

3synthesis methods

Product Name:(4-Oxo-3,4-dihydro-1,5-benzothiazepin-5(2H)-yl)-acetic acid
CAS Number:383187-85-7
Molecular formula:C11H11NO3S
Molecular Weight:237.27

137-07-5
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(4-Oxo-3,4-dihydro-1,5-benzothiazepin-5(2H)-yl)-acetic acid

383187-85-7
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Yield:-

Steps:

Multi-step reaction with 3 steps
1: 220 °C / Microwave irradiation
2: tetrabutylammomium bromide; potassium hydroxide / tetrahydrofuran
3: water; lithium hydroxide / methanol

References:

Wu, Lingyun;Lu, Kai;Desai, Mahesh;Packiarajan, Mathivanan;Joshi, Amita;Marzabadi, Mohammad R.;Jubian, Vrej;Andersen, Kim;Chandrasena, Gamini;Boyle, Noel J.;Walker, Mary W. [Bioorganic and Medicinal Chemistry Letters,2011,vol. 21,# 18,p. 5573 - 5576]

1,5-Benzothiazepine-5(2H)-acetic acid, 3,4-dihydro-4-oxo-, methyl ester (9CI)

913687-69-1
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383187-85-7
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References

53454-43-6 Synthesis

2-thia-6-azabicyclo[5.4.0]undeca-7,9,11-trien-5-one

53454-43-6
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383187-85-7
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References