2,2'-[Dithiobis(3,1-azetidinediyl)]bis[4,5-dihydrothiazole] synthesis

1synthesis methods

Product Name:2,2'-[Dithiobis(3,1-azetidinediyl)]bis[4,5-dihydrothiazole]
CAS Number:384330-54-5
Molecular formula:C12H18N4S4
Molecular Weight:346.56

313468-61-0
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2,2'-[Dithiobis(3,1-azetidinediyl)]bis[4,5-dihydrothiazole]

384330-54-5
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Yield:384330-54-5 93%

Reaction Conditions:

Stage #1: [1-(1,3-thiazolin-2-yl)azetidin-3-yl]thiosulfonic acidwith hydrogenchloride at 55; for 2 h;
Stage #2: with dihydrogen peroxide in methanol at 5; for 0.75 h;

References:

Isoda, Takeshi;Yamamura, Itsuki;Tamai, Satoshi;Kumagai, Toshio;Nagao, Yoshimitsu [Chemical and Pharmaceutical Bulletin,2006,vol. 54,# 10,p. 1408 - 1411]

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