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388594-31-8

Carbamic acid, (4-chloro-5-formyl-2-thiazolyl)-, 1,1-dimethylethyl ester (9CI) synthesis

1synthesis methods
24424-99-5 Synthesis
Di-tert-butyl dicarbonate

24424-99-5
832 suppliers
$13.50/25G

76874-79-8 Synthesis
2-AMINO-4-CHLORO-5-THIAZOLECARBALDEHYDE

76874-79-8
91 suppliers
$10.00/100mg

-

Yield:388594-31-8 87%

Reaction Conditions:

with dmap in 1,4-dioxane at 60; for 2 h;

References:

Masuda, Naoyuki;Yamamoto, Osamu;Fujii, Masahiro;Ohgami, Tetsuro;Fujiyasu, Jiro;Kontani, Toru;Moritomo, Ayako;Orita, Masaya;Kurihara, Hiroyuki;Koga, Hironobu;Nakahara, Hideaki;Kageyama, Shunji;Ohta, Mitsuaki;Inoue, Hiroshi;Hatta, Toshifumi;Suzuki, Hiroshi;Sudo, Kenji;Shimizu, Yasuaki;Kodama, Eiichi;Matsuoka, Masao;Fujiwara, Masatoshi;Yokota, Tomoyuki;Shigeta, Shiro;Baba, Masanori [Bioorganic and Medicinal Chemistry,2004,vol. 12,# 23,p. 6171 - 6182]