2,6-DICHLORO-9-(2-DEOXY-3,5,DI-O-(4-METHYLBENZOYL-BETA-D-ERYTHROPENTOFURANOSYL)-9H-PURINE) synthesis

3synthesis methods

Product Name:2,6-DICHLORO-9-(2-DEOXY-3,5,DI-O-(4-METHYLBENZOYL-BETA-D-ERYTHROPENTOFURANOSYL)-9H-PURINE)
CAS Number:38925-80-3
Molecular formula:C26H22Cl2N4O5
Molecular Weight:541.38

4330-21-6 Synthesis

2-Deoxy-alpha-D-erythropentofuranosyl chloride 3,5-bis(4-methylbenzoate)

4330-21-6
167 suppliers
$7.00/250mg

5451-40-1 Synthesis

5451-40-1
488 suppliers
$10.00/1g

2,6-DICHLORO-9-(2-DEOXY-3,5,DI-O-(4-METHYLBENZOYL-BETA-D-ERYTHROPENTOFURANOSYL)-9H-PURINE)

38925-80-3
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Yield:38925-80-3 78%

Reaction Conditions:

Stage #1: 2,6 dichloropurinewith sodium hydride in tetrahydrofuran;acetonitrile at 20;
Stage #2: 2-deoxy-3,5-di-O-p-toluoyl-α-D-erythro-pentofuranosyl chloride in tetrahydrofuran;acetonitrile at 20; for 16.5 h;

References:

Liu, Fei;Liu, Yingju;Xu, Rui-Gang;Dai, Guifu;Zhao, Liu-Xi;Wang, Yafeng;Liu, Hong-Min;Liu, Feng-Wu;Pannecouque, Christophe;Herdewijn, Piet [Chemistry and biodiversity,2015,vol. 12,# 5,p. 813 - 822]

4330-21-6 Synthesis

4330-21-6
167 suppliers
$7.00/250mg

5451-40-1 Synthesis

5451-40-1
488 suppliers
$10.00/1g

38925-80-3
9 suppliers
inquiry

7H-Purine, 2,6-dichloro-7-[2-deoxy-3,5-bis-O-(4-methylbenzoyl)-β-D-erythro-pentofuranosyl]-

91713-50-7
0 suppliers
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References

4330-21-6 Synthesis

4330-21-6
167 suppliers
$7.00/250mg

5451-40-1 Synthesis

5451-40-1
488 suppliers
$10.00/1g

38925-80-3
9 suppliers
inquiry

91713-50-7
0 suppliers
inquiry

References

2,6-DICHLORO-9-(2-DEOXY-3,5,DI-O-(4-METHYLBENZOYL-BETA-D-ERYTHROPENTOFURANOSYL)-9H-PURINE) Related Search:

2,6-Dichloropurine-2'-deoxyriboside 6-CHLORO-9-(3,5-O-DI(P-TOLUOYL)-BETA-D-2-DEOXYRIBOFURANOSYL) PURINE 2,6-Dichloropurine