ChemicalBook CAS DataBase List (2-amino-4,5-dimethoxyphenyl)-(4-methylphenyl)methanone

(2-amino-4,5-dimethoxyphenyl)-(4-methylphenyl)methanone synthesis

3synthesis methods

Product Name:(2-amino-4,5-dimethoxyphenyl)-(4-methylphenyl)methanone
CAS Number:391251-83-5
Molecular formula:C16H17NO3
Molecular Weight:271.31

91-16-7
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(2-amino-4,5-dimethoxyphenyl)-(4-methylphenyl)methanone

391251-83-5
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Yield:-

Steps:

Multi-step reaction with 3 steps
1: AlCl₃ / benzene / 2.5 h / 55 - 60 °C
2: 68 percent / HNO₃; AcOH / 0.5 h / 0 - 20 °C
3: 73 percent / Fe; AcOH / H₂O; ethyl acetate / 6 h / Heating

References:

Butin, Alexander V.;Smirnov, Sergey K.;Stroganova, Tatyana A.;Bender, Wolfgang;Krapivin, Gennady D. [Tetrahedron,2007,vol. 63,# 2,p. 474 - 491]

(4,5-dimethoxy-2-nitrophenyl)-(4-methylphenyl)methanone

681470-02-0
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391251-83-5
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References

116412-87-4 Synthesis

116412-87-4
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391251-83-5
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References