ChemicalBook CAS DataBase List 2-(TRIFLUOROMETHYL)CYCLOHEXA-2,5-DIENE-1,4-DIONE(WXG00208)

2-(TRIFLUOROMETHYL)CYCLOHEXA-2,5-DIENE-1,4-DIONE(WXG00208) synthesis

9synthesis methods

Product Name:2-(TRIFLUOROMETHYL)CYCLOHEXA-2,5-DIENE-1,4-DIONE(WXG00208)
CAS Number:393-40-8
Molecular formula:C7H3F3O2
Molecular Weight:176.09

98-17-9 Synthesis

98-17-9
422 suppliers
$5.00/10g

2-(TRIFLUOROMETHYL)CYCLOHEXA-2,5-DIENE-1,4-DIONE(WXG00208)

393-40-8
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Yield:-

Steps:

Multi-step reaction with 3 steps
1: 1.) NaNO, HCl, Na₂CO₃, 2.) NaOH / 1.) H₂O, 30 min, 2.) H₂O, 0-5 deg C
2: 47.2 g / Na₂S₂O₄ / H₂O
3: 35 percent / MnO₂ / aq. H₂SO₄ / 2 h / 5 °C

References:

Dieks, Henrik;Senge, Mathias O.;Kirste, Burkhard;Kurreck, Harry [Journal of Organic Chemistry,1997,vol. 62,# 25,p. 8666 - 8680]

887144-94-7 Synthesis

1-TrifluoroMethyl-1,2-benziodoxol-3(1H)-one

887144-94-7
177 suppliers
$19.00/1g

106-51-4 Synthesis

106-51-4
483 suppliers
$10.00/5g

393-40-8
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References

445-04-5 Synthesis

445-04-5
68 suppliers
$43.00/1g

393-40-8
5 suppliers
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References

887144-97-0 Synthesis

1,3-Dihydro-3,3-dimethyl-1-(trifluoromethyl)-1,2-benziodoxole, Tognis Reagent

887144-97-0
163 suppliers
$28.00/250mg

106-51-4 Synthesis

106-51-4
483 suppliers
$10.00/5g

393-40-8
5 suppliers
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References

98-17-9 Synthesis

98-17-9
422 suppliers
$5.00/10g

393-40-8
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4-Cyclopentene-1,3-dione, 2-chloro-2-(trifluoromethyl)-

113281-17-7
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7-Oxabicyclo[4.1.0]hept-3-ene-2,5-dione, 1-(trifluoromethyl)-

113281-22-4
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2-Cyclopentene-1-carboxylic acid, 5-chloro-1-hydroxy-4-oxo-5-(trifluoromethyl)-, trans- (9CI)

113281-18-8
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References