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1,4-Pentadien-3-one, 1,5-bis(4-Methylphenyl)-, (E,E)- synthesis

4synthesis methods
4-Piperidinone, 1-methyl-2,6-bis(4-methylphenyl)-, (2R,6S)-rel-

116222-11-8
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1,4-Pentadien-3-one, 1,5-bis(4-Methylphenyl)-, (E,E)-

39777-55-4
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Yield:39777-55-4 88 % Chromat.

Reaction Conditions:

with selenium(IV) oxide;acetic acid at 100; for 3 h;retro-aza Michael ring opening;

References:

Vijayabaskar;Perumal;Muthusubramanian;Sivasubramanian [Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry,1999,vol. 38,# 8,p. 909 - 913]