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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
399044-23-6

5(1H)-Indolizinone,2,3,8,8a-tetrahydro-,(8aS)-(9CI) synthesis

7synthesis methods
69610-40-8 Synthesis
BOC-L-Prolinol

69610-40-8
389 suppliers
$6.00/5g

5(1H)-Indolizinone,2,3,8,8a-tetrahydro-,(8aS)-(9CI)

399044-23-6
3 suppliers
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-

Yield:-

Steps:

Multi-step reaction with 5 steps
1.1: 89 percent / iodine; imidazole; triphenylphosphine / diethyl ether / 12 h / 20 °C
2.1: CuI / tetrahydrofuran / 0.5 h / -40 - -10 °C
2.2: 87 percent / tetrahydrofuran / 3 h / -40 - 20 °C
3.1: 99 percent / trifluoroacetic acid / CH2Cl2 / 1 h / 0 °C
4.1: 65 percent / Et3N / CH2Cl2 / 3 h / 20 °C
5.1: 74 percent / (1,3-dimesityl-4,5-dihydroimidazol-2-ylidene)Cl2(PCy3)RuCHPh / CH2Cl2 / 3 h / 20 °C

References:

Park, So Hyun;Kang, Hyun Jung;Ko, Sangwon;Park, Soyoung;Chang, Sukbok [Tetrahedron Asymmetry,2001,vol. 12,# 18,p. 2621 - 2624]

2-Propen-1-one, 1-[(2S)-2-(2-propen-1-yl)-1-pyrrolidinyl]-

399044-22-5
0 suppliers
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5(1H)-Indolizinone,2,3,8,8a-tetrahydro-,(8aS)-(9CI)

399044-23-6
3 suppliers
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References
(S)-2-allylpyrrolidine

132959-53-6
2 suppliers
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5(1H)-Indolizinone,2,3,8,8a-tetrahydro-,(8aS)-(9CI)

399044-23-6
3 suppliers
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References
23356-96-9 Synthesis
L-(+)-Prolinol

23356-96-9
458 suppliers
$11.19/5G

5(1H)-Indolizinone,2,3,8,8a-tetrahydro-,(8aS)-(9CI)

399044-23-6
3 suppliers
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References
338945-22-5 Synthesis
(S)-2-IodoMethyl-pyrrolidine-1-carboxylic acid tert-butyl ester

338945-22-5
12 suppliers
$809.00/1g

5(1H)-Indolizinone,2,3,8,8a-tetrahydro-,(8aS)-(9CI)

399044-23-6
3 suppliers
inquiry

References