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ChemicalBook CAS DataBase List (3R,4R)-3-Methoxyoxan-4-amine hydrochloride

(3R,4R)-3-Methoxyoxan-4-amine hydrochloride synthesis

3synthesis methods
624734-17-4 Synthesis
3-methoxy-tetrahydropyran-4-one

624734-17-4
69 suppliers
$33.00/250mg

(3R,4R)-3-Methoxyoxan-4-amine hydrochloride

1232064-63-9
18 suppliers
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Yield:-

Steps:

Multi-step reaction with 3 steps
1: hydrogen / Raney-Nickel / ethanol / 360 h / 3750.38 Torr
2: hydrogen; acetic acid / palladium 10% on activated carbon / methanol / 18 h / 3750.38 Torr
3: hydrogenchloride / diethyl ether

References:

BOEHRINGER INGELHEIM INTERNATIONAL GMBH;EBEL, Heiner;FRATTINI, Sara;GERLACH, Kai;GIOVANNINI, Riccardo;HOENKE, Christoph;SANTAGOSTINO, Marco;SCHEUERER, Stefan;TRIESELMANN, Thomas WO2011/73155, 2011, A1