4-(1-PIPERAZINYL)BENZAMIDE synthesis
- Product Name:4-(1-PIPERAZINYL)BENZAMIDE
- CAS Number:116290-73-4
- Molecular formula:C11H15N3O
- Molecular Weight:205.26
Yield:116290-73-4 82%
Reaction Conditions:
in water at 100;
Steps:
1
Compound 6 (1.40 g, 10.0 mmol) and Compound 7 (4.6 g, 53.1 mmol) were added to water (10 mL) and stirred at 100 ° C overnight. After completion of the reaction, the mixture was cooled to room temperature, and a solid was precipitated, filtered, washed with water, toluene, and dried to give Compound 8 (1.68 g, 82%).
References:
CN108570039,2018,A Location in patent:Paragraph 0123
68104-63-2
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