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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide

4-(2-METHOXYPHENYL)-2-METHYL-1-BUTENE synthesis

10synthesis methods
2-Butanone, 4-(2-methoxyphenyl)-

63449-79-6
1 suppliers
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Methyltriphenylphosphonium bromide

1779-49-3
598 suppliers
$5.00/10g

4-(2-METHOXYPHENYL)-2-METHYL-1-BUTENE

18272-85-0
9 suppliers
$381.00/1g

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Yield:18272-85-0 89%

Reaction Conditions:

Stage #1: Methyltriphenylphosphonium bromidewith sodium t-butanolate in tetrahydrofuran at 0; for 0.5 h;
Stage #2: 4-(o-methoxyphenyl)-butan-2-one in tetrahydrofuran at 20; for 3 h;

References:

Lu, Yanhui;Nakatsuji, Hidefumi;Okumura, Yukimasa;Yao, Lu;Ishihara, Kazuaki [Journal of the American Chemical Society,2018,vol. 140,# 19,p. 6039 - 6043] Location in patent:supporting information

7035-02-1 Synthesis
2-Methoxybenzyl chloride

7035-02-1
106 suppliers
$59.00/10g

3-Chloro-2-methylpropene

563-47-3
243 suppliers
$10.00/5g

4-(2-METHOXYPHENYL)-2-METHYL-1-BUTENE

18272-85-0
9 suppliers
$381.00/1g

References
2-Methyl-4-(2-methoxyphenyl)-2-butanol

56052-48-3
0 suppliers
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Benzene, 1-methoxy-2-(3-methyl-2-buten-1-yl)-

4957-17-9
3 suppliers
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4-(2-METHOXYPHENYL)-2-METHYL-1-BUTENE

18272-85-0
9 suppliers
$381.00/1g

References
529-28-2 Synthesis
2-Iodoanisole

529-28-2
239 suppliers
$8.00/5g

4-(2-METHOXYPHENYL)-2-METHYL-1-BUTENE

18272-85-0
9 suppliers
$381.00/1g

References
3-Butyn-2-ol, 4-(2-methoxyphenyl)-2-methyl-

40904-92-5
0 suppliers
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4-(2-METHOXYPHENYL)-2-METHYL-1-BUTENE

18272-85-0
9 suppliers
$381.00/1g

References

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