4-(2-PROPENYL)-2-CYCLOHEXEN-1-ONE synthesis

4synthesis methods

Product Name:4-(2-PROPENYL)-2-CYCLOHEXEN-1-ONE
CAS Number:4166-61-4
Molecular formula:C9H12O
Molecular Weight:136.19

2-Cyclohexen-1-one, 3-ethoxy-6-(2-propen-1-yl)-

58775-54-5
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4166-61-4
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$215.00/250mg

Yield:4166-61-4 78%

Reaction Conditions:

Stage #1: (+/-)-3-ethoxy-6-(prop-2-enyl)-cyclohex-2-en-1-onewith lithium aluminium tetrahydride in diethyl ether; for 1 h;
Stage #2: with hydrogenchloride in diethyl ether; for 0.5 h;Further stages.;

References:

Huffman, John W.;Thompson, Alicia L.S.;Wiley, Jenny L.;Martin, Billy R. [Bioorganic and Medicinal Chemistry,2008,vol. 16,# 1,p. 322 - 335]

Cyclopentene, 3-(2-propen-1-yl)-1-[(trimethylsilyl)oxy]-

153788-35-3
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4166-61-4
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References

1,4-Dioxaspiro[4.5]dec-7-ene, 8-(phenylsulfonyl)-

81841-89-6
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4166-61-4
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1,4-Dioxaspiro[4.5]dec-6-ene, 8-(phenylsulfonyl)-8-(2-propenyl)-

81841-92-1
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4166-61-4
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81842-16-2
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References

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