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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
104958-55-6

4-(3,3,3-Trifluoropropyl)benzoic acid synthesis

1synthesis methods
Benzoic acid, 4-(heptafluoropropyl)-

88950-94-1
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4-(3,3,3-Trifluoropropyl)benzoic acid

104958-55-6
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Yield:104958-55-6 30%

Reaction Conditions:

with sodium hydroxide;hydrogen;nickel in methanol at 20; for 7 h;

References:

Fialkov, Yu. A.;Zalesskaya, I. M.;Shelyazhenko, S. V.;Yagupol'skii, L. M. [Journal of Organic Chemistry USSR (English Translation),1985,vol. 21,# 11,p. 2201 - 2205][Zhurnal Organicheskoi Khimii,1985,vol. 21,# 11,p. 2407 - 2411]