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ChemicalBook CAS DataBase List 4-(3-BROMO-BENZYLOXY)-BENZALDEHYDE

4-(3-BROMO-BENZYLOXY)-BENZALDEHYDE synthesis

3synthesis methods
-

Yield:588676-02-2 79%

Reaction Conditions:

Stage #1: 4-hydroxy-benzaldehydewith potassium carbonate in N,N-dimethyl-formamide at 20; for 0.0833333 h;Inert atmosphere;
Stage #2: 1-bromo-3-(bromomethyl)benzene in N,N-dimethyl-formamide at 20 - 60;Inert atmosphere;

References:

Woo, Jacqueline C.S.;Cui, Sheng;Walker, Shawn D.;Faul, Margaret M. [Tetrahedron,2010,vol. 66,# 26,p. 4730 - 4737] Location in patent:experimental part