4-(3-methyl-1,2,4-oxadiazol-5-yl)aniline synthesis

2synthesis methods

Product Name:4-(3-methyl-1,2,4-oxadiazol-5-yl)aniline
CAS Number:76635-31-9
Molecular formula:C9H9N3O
Molecular Weight:175.19

122-04-3
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$15.00/1g

4-(3-methyl-1,2,4-oxadiazol-5-yl)aniline

76635-31-9
27 suppliers
$45.00/25mg

Yield:-

Steps:

Multi-step reaction with 3 steps
1: N-ethyl-N,N-diisopropylamine; hydroxylamine / ethanol; acetonitrile / 1 h / 90 °C
2: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C
3: acetic acid; iron / 5 h / 20 °C

References:

Sumitomo Dainippon Pharma Co., Ltd.;IKUMA Yohei;FUKUDA Nobuhisa;IWATA Masato;KIMURA Hidenori;SUZUKI Kuniko EP2876105, 2015, A1

3-Methyl-5-(4-nitrophenyl)-1,2,4-oxadiazole

1455-82-9
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76635-31-9
27 suppliers
$45.00/25mg

References

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4-(3-phenyl-1,2,4-oxadiazol-5-yl)aniline