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ChemicalBook CAS DataBase List 4,4'-(1,10-Phenanthroline-2,9-diyl)diphenol
88498-43-5

4,4'-(1,10-Phenanthroline-2,9-diyl)diphenol synthesis

12synthesis methods
89333-97-1 Synthesis
2,9-bis(4-methoxyphenyl)-1,10-phenanthroline

89333-97-1
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Yield:88498-43-5 100%

Reaction Conditions:

Stage #1: 2,9-bis-(4-methoxy-phenyl)-1,10-phenanthrolinewith pyridine hydrochloride at 220; for 6 h;
Stage #2: with water in ethanol at 20; for 1 h;

References:

Amir, Faheem;Barnes, Jonathan C.;Chang, Christy;Colley, Nathan D.;Fisher, Jeremy M.;Greene, Angelique F.;Li, Lei;Li, Ruihan;Li, Xuesong;Nosiglia, Mark A. [Inorganic Chemistry,2020] Location in patent:supporting information