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ChemicalBook CAS DataBase List 4,4',4'',4'''-silanetetrayltetrabenzaldehyde

4,4',4'',4'''-silanetetrayltetrabenzaldehyde synthesis

1synthesis methods
24856-58-4 Synthesis
4-BROMOBENZALDEHYDE DIMETHYL ACETAL

24856-58-4
86 suppliers
$10.00/1g

4,4',4'',4'''-silanetetrayltetrabenzaldehyde

1055999-34-2
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Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -65 °C / Inert atmosphere
1.2: 870 min / -65 - 20 °C / Inert atmosphere
2.1: hydrogenchloride / tetrahydrofuran; water / 2 h / Reflux

References:

WO2022/254902,2022,A1

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