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4,4,5,5-Tetramethyl-1,3-dioxolan-2-one synthesis

9synthesis methods
Carbamic acid, ethyl-, 2-hydroxy-1,1,2-trimethylpropyl ester (9CI)

743477-27-2
3 suppliers
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2018-61-3 Synthesis
N-Acetyl-L-phenylalanine

2018-61-3
377 suppliers
$14.00/5G

4,4,5,5-Tetramethyl-1,3-dioxolan-2-one

19424-29-4
1 suppliers
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2361-96-8 Synthesis
AC-PHE-OET

2361-96-8
97 suppliers
$7.00/250mg

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Yield:2361-96-8 100%

Reaction Conditions:

with tert.-butylnitrite;3 A molecular sieve in dichloromethane at 60; for 12 h;

References:

Suzuki, Masumi;Sugai, Takeshi [Bulletin of the Chemical Society of Japan,2004,vol. 77,# 6,p. 1217 - 1228]