ChemicalBook CAS DataBase List 4,4,6-TRIMETHYL-2-VINYL-1,3,2-DIOXABORINANE

4,4,6-TRIMETHYL-2-VINYL-1,3,2-DIOXABORINANE synthesis

6synthesis methods

Product Name:4,4,6-TRIMETHYL-2-VINYL-1,3,2-DIOXABORINANE
CAS Number:4627-10-5
Molecular formula:C8H15BO2
Molecular Weight:154.01

107-41-5
487 suppliers
$5.00/100g

1826-67-1
210 suppliers
$60.89/100ml

4,4,6-TRIMETHYL-2-VINYL-1,3,2-DIOXABORINANE

4627-10-5
33 suppliers
$831.95/5G

Yield:4627-10-5 82%

Reaction Conditions:

Stage #1: vinyl magnesium bromidewith Trimethyl borate in tetrahydrofuran at -78; for 1 h;
Stage #2: with hydrogenchloride in tetrahydrofuran;diethyl ether at 20; for 0.166667 h;
Stage #3: 2-methyl-2,4-pentanediol in tetrahydrofuran;diethyl ether at 20; for 1 h;

References:

Lightfoot, Andrew P.;Twiddle, Steven J.R.;Whiting, Andrew [Organic and Biomolecular Chemistry,2005,vol. 3,# 17,p. 3167 - 3172]

107-41-5
487 suppliers
$5.00/100g