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ChemicalBook CAS DataBase List 4,4'-Bis(diethylmethylphosphonate)-2,2'-bipyridine
176220-38-5

4,4'-Bis(diethylmethylphosphonate)-2,2'-bipyridine synthesis

11synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: 89 percent / NaBH4 / ethanol / 3 h / 20 °C
2: 88 percent / HBr; H2SO4 / 6 h / Heating
3: 73 percent / 3 h / Heating

References:

Will, Geoffrey;Boschloo, Gerrit;Rao, S. Nagaraja;Fitzmaurice, Donald [Journal of Physical Chemistry B,1999,vol. 103,# 38,p. 8067 - 8079]

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