4-(4-Butylphenylazo)phenol synthesis
1synthesis methods
- Product Name:4-(4-Butylphenylazo)phenol
- CAS Number:103939-81-7
- Molecular formula:C16H18N2O
- Molecular Weight:254.33
Yield:103939-81-7 94%
Reaction Conditions:
Stage #1: 4-Butylanilinewith hydrogenchloride;sodium nitrite in water;acetone at 2; for 0.333333 h;Cooling with ice;
Stage #2: phenolwith sodium carbonate;sodium hydroxide in water;acetone at 8;Cooling with ice;
References:
Houston, Judith E.;Kelly, Elaine A.;Kruteva, Margarita;Chrissopoulou, Kiriaki;Cowieson, Nathan;Evans, Rachel C. [Journal of Materials Chemistry C,2019,vol. 7,# 35,p. 10945 - 10952] Location in patent:supporting information