4,4'-DIMETHOXY-3''-METHYLTRITYL ALCOHOL synthesis
1synthesis methods
- Product Name:4,4'-DIMETHOXY-3''-METHYLTRITYL ALCOHOL
- CAS Number:541540-97-0
- Molecular formula:C22H22O3
- Molecular Weight:334.41
Yield:541540-97-0 81%
Reaction Conditions:
Stage #1: 1-bromo-4-methoxy-benzenewith magnesium in tetrahydrofuran at 20; for 1 h;
Stage #2: 1-methoxycarbonyl-3-methylbenzene in tetrahydrofuran at 0 - 20; for 1 h;
References:
Seio, Kohji;Kumura, Kou;Bologna, Jean-Charles;Sekine, Mitsuo [Journal of Organic Chemistry,2003,vol. 68,# 10,p. 3849 - 3859]