4,4'-DIMETHYL-D6-DIPHENYL synthesis
- Product Name:4,4'-DIMETHYL-D6-DIPHENYL
- CAS Number:42052-87-9
- Molecular formula:C14H8D6
- Molecular Weight:188.3
1667-10-3
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Yield:42052-87-9 82%
Reaction Conditions:
Stage #1: 4,4'-bis(chloromethyl)biphenylwith triphenylphosphine in tetrahydrofuran at 50 - 60; for 48 h;
Stage #2: with potassium cyanide;water-d2 in tetrahydrofuran at 40 - 50; for 14 h;
References:
Lee, Ka Young;Na, Jeong Eun;Lee, Mi Jung;Kim, Jae Nyoung [Tetrahedron Letters,2004,vol. 45,# 31,p. 5977 - 5981]
613-33-2
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