ChemicalBook CAS DataBase List 4-[5-(3-Hydroxyphenyl)-2-thienyl]-2-methylphenol

4-[5-(3-Hydroxyphenyl)-2-thienyl]-2-methylphenol synthesis

1synthesis methods

Product Name:4-[5-(3-Hydroxyphenyl)-2-thienyl]-2-methylphenol
CAS Number:1122660-25-6
Molecular formula:C17H14O2S
Molecular Weight:282.36

2-(4-Methoxy-3-Methylphenyl)-5-(3-Methoxyphenyl)thiophene

1193525-42-6
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4-[5-(3-Hydroxyphenyl)-2-thienyl]-2-methylphenol

1122660-25-6
33 suppliers
$225.00/100mg

Yield:1122660-25-6 79%

Reaction Conditions:

with boron tribromide in dichloromethane at -78 - 20;Inert atmosphere;

References:

Bey, Emmanuel;Marchais-Oberwinkler, Sandrine;Negri, Matthias;Kruchten, Patricia;Oster, Alexander;Klein, Tobias;Spadaro, Alessandro;Werth, Ruth;Frotscher, Martin;Birk, Barbara;Hartmann, Rolf W. [Journal of Medicinal Chemistry,2009,vol. 52,# 21,p. 6724 - 6743] Location in patent:experimental part