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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide

4,5-dichloro-2-nitrobenzonitrile synthesis

1synthesis methods
143-33-9 Synthesis
Sodium cyanide

143-33-9
5 suppliers
$10.00/1g

6641-64-1 Synthesis
4,5-Dichloro-2-nitroaniline

6641-64-1
211 suppliers
$6.00/5g

4,5-dichloro-2-nitrobenzonitrile

28523-93-5
9 suppliers
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Yield:-

Reaction Conditions:

with tert.-butylnitrite;boron trifluoride diethyl etherate1.) THF, CH2Cl2, -10 deg C, 2.) H2O, rt, overnight;Yield given;Multistep reaction;

References:

Zhu, Zhijian;Lippa, Blaise;Townsend, Leroy B. [Journal of Organic Chemistry,1999,vol. 64,# 11,p. 4159 - 4168]