4,6-bis(3,5-dichlorophenyl)-2-methylpyrimidine synthesis
- Product Name:4,6-bis(3,5-dichlorophenyl)-2-methylpyrimidine
- CAS Number:1030380-50-7
- Molecular formula:C17H10Cl4N2
- Molecular Weight:384.09
1780-26-3
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Yield:1030380-50-7 81%
Reaction Conditions:
with bis-triphenylphosphine-palladium(II) chloride;sodium carbonate in water;acetonitrile at 60; for 6 h;Inert atmosphere;Suzuki-Miyaura coupling reaction;
References:
Sasabe, Hisahiro;Tanaka, Daisaku;Yokoyama, Daisuke;Chiba, Takayuki;Pu, Yong-Jin;Nakayama, Ken-Ichi;Yokoyama, Masaaki;Kido, Junji [Advanced Functional Materials,2011,vol. 21,# 2,p. 336 - 342] Location in patent:experimental part