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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide

4,8-dioxaundecane-1,11-diol synthesis

10synthesis methods
Propanoic acid, 3,3'-[1,3-propanediylbis(oxy)]bis-, diethyl ester (9CI)

354117-85-4
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4,8-dioxaundecane-1,11-diol

4161-32-4
17 suppliers
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Yield:4161-32-4 79%

Reaction Conditions:

Stage #1: C13H24O6with lithium aluminium tetrahydride
Stage #2: with water

Steps:



Compound 97 (4,8-dioxaundecane-l,ll-diol) was synthesized in three steps using established methods[33] as shown in Figure 12 - Scheme 12: (a) acrylonitrile, 2%w/v sodium hydroxide; (b) cone, sulfuric acid, 95% ethanol; (c) lithium aluminium hydride.

References:

WO2009/152392,2009,A2 Location in patent:Page/Page column 25

1,3-Dioxane, 2,2'-methylenebis-

30963-84-9
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4,8-dioxaundecane-1,11-diol

4161-32-4
17 suppliers
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References
2,6,10,14-Tetraoxapentadecane, 1,15-diphenyl-

1167572-50-0
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4,8-dioxaundecane-1,11-diol

4161-32-4
17 suppliers
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References
504-63-2 Synthesis
1,3-Propanediol

504-63-2
525 suppliers
$9.00/5g

4,8-dioxaundecane-1,11-diol

4161-32-4
17 suppliers
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2396-61-4 Synthesis
3,3'-oxydipropanol

2396-61-4
34 suppliers
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1-Propanol,3,3'-[oxybis(3,1-propanediyloxy)]bis- (9CI)

30242-05-8
9 suppliers
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3-[3-[3-[3-[3-(3-hydroxypropoxy)propoxy]propoxy]propoxy]propoxy]propan-1-ol

55333-98-7
4 suppliers
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1167572-53-3

1167572-53-3
4 suppliers
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69039-85-6 Synthesis
69039-85-6

69039-85-6
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References
2H-Pyran, 2,2'-[1,3-propanediylbis(oxy-3,1-propanediyloxy)]bis[tetrahydro- (9CI)

92818-31-0
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4,8-dioxaundecane-1,11-diol

4161-32-4
17 suppliers
inquiry

References