4-AMINO-6-METHYL (1H)INDAZOLE synthesis
- Product Name:4-AMINO-6-METHYL (1H)INDAZOLE
- CAS Number:90764-89-9
- Molecular formula:C8H9N3
- Molecular Weight:147.18
106-42-3
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Yield:-
Steps:
Multi-step reaction with 4 steps
1: sulfuric acid; potassium nitrate / 2 h / 20 °C / Inert atmosphere
2: iron; hydrogenchloride / methanol; water; 1,4-dioxane / 80 °C / Inert atmosphere
3: sodium nitrite; acetic acid / water / Inert atmosphere
4: iron; ammonium chloride / ethanol; water / 80 °C / Inert atmosphere
References:
Ning, Xiang-Li;Li, Yu-Zhi;Huo, Cui;Deng, Ji;Gao, Cheng;Zhu, Kai-Rong;Wang, Miao;Wu, Yu-Xiang;Yu, Jun-Lin;Ren, Ya-Li;Luo, Zong-Yuan;Li, Gen;Chen, Yang;Wang, Si-Yao;Peng, Cheng;Yang, Ling-Ling;Wang, Zhou-Yu;Wu, Yong;Qian, Shan;Li, Guo-Bo [Journal of Medicinal Chemistry,2021,vol. 64,# 12,p. 8303 - 8332]
609-92-7
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62564-50-5
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857773-68-3
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