4-AMINOPIPERIDINE-4-CARBOXYLIC ACID HYDROBROMIDE synthesis

2synthesis methods

Product Name:4-AMINOPIPERIDINE-4-CARBOXYLIC ACID HYDROBROMIDE
CAS Number:76508-55-9
Molecular formula:C6H13BrN2O2
Molecular Weight:225.09

29976-54-3 Synthesis

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4-AMINOPIPERIDINE-4-CARBOXYLIC ACID HYDROBROMIDE

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Yield:-

Steps:

Multi-step reaction with 2 steps
1: 77 percent / aq. ammonia, ammonium chloride / H₂O / 5 h / 60 °C
2: 1.) conc. HCl, 2.) conc. HBr / 1.) water, 24 deg C, 2 d, 2.) reflux, 4 h

References:

Jacobsen;Schaumburg;Krogsgaard-Larsen [Acta chemica Scandinavica. Series B: Organic chemistry and biochemistry,1980,vol. 34,# 5 B,p. 319 - 326]

1-Piperidinecarboxylic acid, 4-amino-4-cyano-, methyl ester

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76508-55-9
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References