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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
ChemicalBook CAS DataBase List 4-benzylcyclohexanone
35883-77-3

4-benzylcyclohexanone synthesis

10synthesis methods
69225-59-8 Synthesis
1,4-Cyclohexanedione mono(2,2-dimethyltrimethylene ketal)

69225-59-8
206 suppliers
$8.00/1g

1589-82-8 Synthesis
BENZYLMAGNESIUM BROMIDE

1589-82-8
156 suppliers
$60.00/5g

4-benzylcyclohexanone

35883-77-3
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Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: zinc(II) chloride / diethyl ether; tetrahydrofuran / 2.5 h / 0 °C
2.1: toluene-4-sulfonic acid / toluene / Reflux; Dean-Stark
2.2: 5 h / 20 °C
2.3: 14.5 h / 0 - 20 °C

References:

Taisho Pharmaceutical Co., Ltd.;TAKAYAMA, Tetsuo;SHIBATA, Tsuyoshi;SHIOZAWA, Fumiyasu;KAWABE, Kenichi;SHIMIZU, Yuki;HAMADA, Makoto;HIRATATE, Akira;TAKAHASHI, Masato;USHIYAMA, Fumihito;OI, Takahiro;SHIRASAKI, Yoshihisa;MATSUDA, Daisuke;KOIZUMI, Chie;KATO, Sota EP2881384, 2015, A1

8-benzyl-1,4-dioxaspiro[4.5]decane

83631-88-3
0 suppliers
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4-benzylcyclohexanone

35883-77-3
20 suppliers
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References
1530-39-8 Synthesis
(4-CHLOROBENZYL)TRIPHENYLPHOSPHONIUM CHLORIDE

1530-39-8
92 suppliers
$15.00/1g

4-benzylcyclohexanone

35883-77-3
20 suppliers
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References
Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-

1000210-73-0
0 suppliers
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4-benzylcyclohexanone

35883-77-3
20 suppliers
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References
Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-

1000210-73-0
0 suppliers
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4-benzylcyclohexanone

35883-77-3
20 suppliers
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2-Cyclohexen-1-one, 4-(phenylmethyl)-

81842-24-2
2 suppliers
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References