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ChemicalBook CAS DataBase List (4-BENZYLOXYBUTYL)TRIPHENYLPHOSPHONIUM BROMIDE
85514-52-9

(4-BENZYLOXYBUTYL)TRIPHENYLPHOSPHONIUM BROMIDE synthesis

2synthesis methods
-

Yield:85514-52-9 47%

Reaction Conditions:

Stage #1: 4-bromobutyl benzyl ether;triphenylphosphine in acetonitrile; for 164 h;Reflux;
Stage #2: with potassium hydroxide in tetrahydrofuran;water; for 3.5 h;

References:

Gresser, Mary J.;Keller, Paul A.;Wales, Steven M. [Tetrahedron Letters,2009,vol. 50,# 34,p. 4899 - 4902] Location in patent:scheme or table

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