4-[Bis(9,9-dimethylfluoren-2-yl)amino]azobenzene synthesis
- Product Name:4-[Bis(9,9-dimethylfluoren-2-yl)amino]azobenzene
- CAS Number:883554-70-9
- Molecular formula:C42H35N3
- Molecular Weight:581.75
60-09-3
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$17.67/1gm:
144981-85-1
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$7.00/1g
883554-70-9
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$391.00/200mg
Yield:883554-70-9 60%
Reaction Conditions:
with 18-crown-6 ether;copper;potassium carbonate in 1,3,5-trimethyl-benzene; for 35 h;Inert atmosphere;Reflux;Ullmann reaction;
References:
Tanino, Takahiro;Yoshikawa, Satoru;Ujike, Toshiki;Nagahama, Daisuke;Moriwaki, Kazuyuki;Takahashi, Toru;Kotani, Yoshiko;Nakano, Hideyuki;Shirota, Yasuhiko [Journal of Materials Chemistry,2007,vol. 17,# 47,p. 4953 - 4963] Location in patent:experimental part