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4-Boc-3-methoxy-morpholine synthesis

5synthesis methods
-

Yield:195964-53-5 80%

Reaction Conditions:

Stage #1: 4-(tert-butoxycarbonyl)morpholine-3-carboxylic acidwith potassium hydroxide in methanol;Sonication;
Stage #2: methanol at 20;Electrochemical reaction;

References:

López, Enol;van Melis, Carlo;Martín, Raúl;Petti, Alessia;de la Hoz, Antonio;Díaz-Ortíz, ángel;Dobbs, Adrian P.;Lam, Kevin;Alcázar, Jesús [Advanced Synthesis and Catalysis,2021,vol. 363,# 19,p. 4521 - 4525] Location in patent:supporting information